Author

Ayan Barua

Date of Award

2024

Document Type

Thesis

Degree Name

Master of Science (MS)

Department

Chemistry

Committee Chair

Bernhard Vogler

Committee Member

Olaf Nachtigall

Committee Member

Sharifa Love-Rutledge

Research Advisor

Bernhard Vogler

Subject(s)

Metabolites--Analysis, Mass spectrometry

Abstract

This research aims to establish advanced analytical methods for targeted metabolomics using Gas-Chromatography-Mass Spectrometry (GC-MS). The focus is on quantifying key metabolites involved in specific metabolic pathways, optimizing sample preparation, and ensuring rigorous validation of method development parameters. By targeting thirteen specific metabolites, the research seeks to enhance metabolite extraction efficiency and analytical sensitivity. Analytical parameters such as selectivity, specificity, range, limit of detection, and limit of quantification were evaluated. This study's findings will contribute to a more precise understanding of metabolic alterations in disease states and improve the robustness of GC-MS-based metabolomics.

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